in neat (no solvent) in vacuo or under inert gas, heated at 240°C for 5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, p. 1542 - 1547
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 30, p. 1874 - 1879
in neat (no solvent) byproducts: Cr, Cr(CO)6, CO; in vacuo or under inert gas, heated at 230°C for 5 h; washed (benzene); TLC;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, p. 1542 - 1547
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 30, p. 1874 - 1879
in neat (no solvent) byproducts: 2,6,2',6'-tetramethyldiphenoquinone; heated for 1 h at 220°C in a glass evacuated ampoule; sepd. by chromy. on silica gel; eluted with petroleum ether;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 6 p. 867 - 872
in toluene byproducts: NaCl, [S2CNEt2]2; mixt. of Sb-complex and ligand in toluene was heated for 3 h at 100°C; solvent was removed, crystd. from hexane, dissolved in hexane, chromd. on alumina column, eluted with hexane;
参考文献
Russian Journal of General Chemistry, , vol. 72, # 9 p. 1379 - 1382
