Effendy; Grigsby, Warren J.; Hart, Robert D.; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Australian Journal of Chemistry, 1997 , vol. 50, # 6 p. 675 - 681
1: tri-phenyl-antimony With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 1,4-bis(2-(trimethysilyl)ethynyl)-benzene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
1: tri-phenyl-antimony With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 4-(trimethylsilyl)-3-butyn-2-one With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
in tetrahydrofuran; 1,4-dioxane
1:1 ratio, 82.3+/-0.2°C;
参考文献
Benlian, D.; Bigorgne, M.
Bulletin de la Societe Chimique de France, 1963 , p. 1583 - 1588
Full Text Show Details
Gmelin Handbook: Sb: Org.Comp.1, 1.1.1.1.6.4.4, page 55 - 78
THF in tetrahydrofuran
Irradiation (UV/VIS); N2-atmosphere; photolysis of hexacaronyl, addn. of ligand; evapn., sublimation off of unreacted hexacarbonyl (60°C, vac.), washing (cold hexane), chromy. (SiO2, hexane), recrystn. (hexane);
参考文献
Aroney, Manuel J.; Buys, Irmi E.; Davies, Murray S.; Hambley, Trevor W.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 19 p. 2827 - 2834
