反应条件
tert.-butylhydroperoxide in diethyl ether
byproducts: t-BuOH, H2O; t-BuOOH was added dropwise to stirred cold (5-10°C) soln. of Sb-compound and acid in Et2O, kept in the dark for 24 h at room temp.; solvent was distilled off under reduced pressure, recrystd. from CHCl3/hexane;
参考文献
Moiseev, Dmitry V.; Gushchin, Aleksey V.; Shavirin, Andrey S.; Kursky, Yury A.; Dodonov, Viktor A.
Journal of Organometallic Chemistry, 2003 , vol. 667, # 1-2 p. 176 - 184
