反应条件
2,2'-azo-bisisobutyronitrile in toluene Ar-atmosphere; 10 molpercent AIBN, equimolar amts. of stibane and alkyne, 90°C, 16 h; solvent removal (vac.), chromy. (SiO2, AcOEt/hexane=1:6); isomer mixt. not sepd., detd. by (1)H-NMR spectroscopy; product contg. 40percent SbPh3;
参考文献
Journal of Organometallic Chemistry, , vol. 571, # 2 p. 297 - 303