4,4,4-三羟基三甲苯合成路线 (共 19 条)
反应条件
chloro-trimethyl-silane; bismuth sulphate in dichloromethane T=20°C; Friedel-Crafts reaction; 12 h;
参考文献
Liu, Cong-Rong; Li, Man-Bo; Yang, Cui-Feng; Tian, Shi-Kai
Chemical Communications, 2008 , # 10 p. 1249 - 1251
反应条件
3,5,5-trimethyl-2-morpholinon-3-yl in dimethylsulfoxide-d6 T=50°C; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 103, # 4 p. 849 - 856
反应条件
toluene-4-sulfonic acid in tetrahydrofuran
反应条件
ethyl mercaptan sodium salt in N,N-dimethyl-formamide 24 h; Heating;
参考文献
Berscheid, Ralf; Nieger, Martin; Voegtle, Fritz
Chemische Berichte, 1992 , vol. 125, # 7 p. 1687 - 1696
反应条件
zinc(II) chloride T=135°C;
参考文献
Journal of the American Chemical Society, , vol. 47, p. 209
反应条件
sodium tetrahydroborate; acetic acid in ethanol
参考文献
Astakhova, I. Kira; Santhosh Kumar; Campbell, Meghan A.; Ustinov, Alexey V.; Korshun, Vladimir A.; Wengel, Jesper
Chemical Communications, 2013 , vol. 49, # 5 p. 511 - 513
反应条件
sulfuric acid; acetic acid
参考文献
Journal of the Chemical Society, , p. 985,988
反应条件
hydrogen fluoride; boron trifluoride T=45°C; P=37503.8 - 60006 Torr; 4.5 h; Product distribution; Further Variations:Reagentstime;
参考文献
Synthesis, , # 15 p. 2543 - 2550
反应条件
1: 51 percent 2: 93 percent / NaSEt / dimethylformamide / 24 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 414 - 416
反应条件
1: 51 percent 2: 93 percent / NaSEt / dimethylformamide / 24 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 414 - 416