in diethyl ether
reaction at -40 to -30°C and boiling on reflux for 2 h;;
参考文献
Neumann, W. P.; Niermann, H.; Sommer, R.
Liebigs Annalen der Chemie, 1962 , vol. 659, p. 27 - 39
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.6, page 110 - 113
in not given
reaction at -40°C and then for 30 min at 0°C;;
参考文献
Neumann, W. P.; Niermann, H.; Sommer, R.
Liebigs Annalen der Chemie, 1962 , vol. 659, p. 27 - 39
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.6, page 110 - 113
Sawyer et al.
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 192
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.7, page 62 - 63
