1-溴-2-(2-丙烯-1-基氧基)-苯合成路线 （共 50 条）
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in hexane
T=-33 - 50°C; Irradiation;
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 464 - 465
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
0.5 h; Heatingother solvent (benzene), other time (5 h); reactions of allyl o-bromoaryl ethers, N-allyl o-bromoacetanilide and related compounds with tributyltin hydride in the presence of activated olefins; Product distribution;
参考文献
Togo, Hideo; Kikuchi, Osamu
Heterocycles, 1989 , vol. 28, # 1 p. 373 - 381
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20 - 24°C; 22 h; LiAlD4, var. time, ratios, without oxygen, further irradiation in the presence of di-t-butyl peroxide; MechanismProduct distribution;
参考文献
Beckwith, Athelstan L. J.; Goh, Swee Hock
Journal of the Chemical Society, Chemical Communications, 1983 , # 16 p. 905 - 906
反应条件
sodium naphthalenide in tetrahydrofuran
Ambient temperaturevarious molar ratio; Product distribution;
参考文献
Do, Sang Rok; Shine, Henry J.
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5414 - 5418
反应条件
1: With zinc in tetrahydrofuran
Heating;
2: With (3,5-dinitrophenyl)(4-methylpiperazin-1-yl)methanone; copper(I) bromide dimethylsulfide complex in N,N-dimethyl acetamide
T=22°C; 1 h;
参考文献
Su, Xianbin; Fox, David J.; Blackwell, David T.; Tanaka, Kiyotaka; Spring, David R.
Chemical Communications, 2006 , # 37 p. 3883 - 3885
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20 - 24°C; 22 h; LiAlD4, var. time, ratios, without oxygen, further irradiation in the presence of di-t-butyl peroxide; MechanismProduct distribution;
参考文献
Beckwith, Athelstan L. J.; Goh, Swee Hock
Journal of the Chemical Society, Chemical Communications, 1983 , # 16 p. 905 - 906
反应条件
1: 100 percent / Et2AlCl / hexane / 2.5 h / 20 °C
2: 85 percent / K2CO3 / acetone / Heating
View Scheme
参考文献
Bagley; Moody; Pepper
Tetrahedron Letters, 2000 , vol. 41, # 35 p. 6901 - 6904
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in hexane
T=-33 - 50°C; Irradiation;
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 464 - 465
反应条件
tetra-n-butylammonium tetrafluoroborate; Ni(cyclam)Br2 in N,N-dimethyl-formamide
T=20°C; Carboxylation; cyclization; P=760 Torr; ElectrolysisMg/Ni electrodes; Product distribution; Further Variations:CatalystsPressuresReaction partnersnature of the electrodes;
参考文献
Olivero; Dunach
European Journal of Organic Chemistry, 1999 , # 8 p. 1885 - 1891
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
T=0°C; Electrolysis;
参考文献
Senboku, Hisanori; Michinishi, Jun-Ya; Hara, Shoji
Synlett, 2011 , # 11 p. 1567 - 1572
