1-甲基-2,4(1h,3h)-喹唑啉二酮合成路线 (共 12 条)
反应条件
acetic acid; sodium hydroxide in water T=40 - 75°C;
参考文献
Prashanth; Madaiah; Revanasiddappa; Veeresh
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 110, p. 324 - 332
反应条件
in N,N-dimethyl acetamide 0.025 h; microwave irradiation;
参考文献
Nikpour, Farzad; Paibast, Touraj
Chemistry Letters, 2005 , vol. 34, # 10 p. 1438 - 1439
反应条件
in N,N-dimethyl acetamide 0.05 h; microwave irradiation;
参考文献
Nikpour, Farzad; Paibast, Touraj
Chemistry Letters, 2005 , vol. 34, # 10 p. 1438 - 1439
反应条件
in diethylene glycol dimethyl ether 1 h; Heating;
参考文献
Barbuch, Robert J.; Peet, Norton P.
Organic Mass Spectrometry, 1988 , vol. 23, p. 816 - 820
反应条件
ethanol T=100 - 120°C; im Rohr;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 39, p. 142
反应条件
1: 54 percent / concentrated ammonium hydroxyde / ethanol / Heating 2: 28 percent / bis-(2-methoxy-ethyl) ether / 1 h / Heating View Scheme
参考文献
Organic Mass Spectrometry, , vol. 23, p. 816 - 820
反应条件
1: sodium hydroxide / water; methanol / 1 h / 60 °C 2: 5 h / 150 °C View Scheme
参考文献
Medicinal Chemistry Research, , vol. 23, # 5 p. 2169 - 2177
反应条件
1.1: sodium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C 1.2: 8 h / 20 - 50 °C 2.1: sodium hydroxide / water; methanol / 1 h / 60 °C 3.1: 5 h / 150 °C View Scheme
参考文献
Medicinal Chemistry Research, , vol. 23, # 5 p. 2169 - 2177
参考文献
Ashirmatov; Urakov; Shakhidoyatov
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 708 - 711
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 39, p. 142