2,3,4,6-四-o-乙酰基-alpha-d-吡喃葡萄糖苷甲酯合成路线 (共 100 条)
参考文献
Carbohydrate Research, , vol. 265, # 1 p. 1 - 8
反应条件
methanol; toluene-4-sulfonic acid anschl. mit Acetanhydrid und Pyridin;
参考文献
Chemische Berichte, , vol. 90, p. 2094
反应条件
sulfuric acid 1.) reflux; 2.) pyridine, rt.; Multistep reaction;
参考文献
Tetrahedron, , vol. 43, # 22 p. 5261 - 5274
反应条件
bis(tri-n-butyltin)oxide 1) toluene, reflux, 4 h, 2) r.t., 18 h; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 241, p. 295 - 299
反应条件
pyridine; air; 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride 1.) toluene, 60 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 35, # 44 p. 8163 - 8166
参考文献
Journal of the Chemical Society, , p. 2976,2978
反应条件
pyridine; [NO][PF6]; sodium methylate Multistep reaction;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
反应条件
sulfuric acid 1.) MeOH, reflux, 6h; 2.) pyridine, rt., 14h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 43, # 22 p. 5275 - 5280
反应条件
pyridine; 1,1,1,3,3,3-hexachloro-propan-2-one 1.) DMF, r.t., 3 d; 2.) 12 h; Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 138, p. 143 - 147
反应条件
pyridine; [NO][PF6]; sodium methylate Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164