2,3,4,6-四-o-乙酰基-alpha-d-吡喃葡萄糖苷甲酯合成路线 (共 100 条)
反应条件
pyridine 1.) DMF, r.t., 3 d; 2.) 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 138, p. 143 - 147
反应条件
pyridine; sulfuric acid 1) reflux, 14 h, 2) room temperature, 14 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 10 p. 2893 - 2896
反应条件
pyridine; sodium methylate Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 2 p. 157 - 164
反应条件
in methanol; acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.34 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
反应条件
in methanol; acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.20 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
参考文献
Tetrahedron, , vol. 45, # 12 p. 3897 - 3906
反应条件
in acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.20 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
反应条件
in acetonitrile electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiClO4 as supporting electrolyte, constant potential 1.34 V (vs standard calomel reference electrode); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236
反应条件
pyridine; iodine 1) reflux, 40 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, , vol. 115, # 2 p. 133 - 139
反应条件
1.) electrochemical synthesis: one compartment, three-electrode, air-tight cell, Pt anode and catode, 0.2 M LiClO4 in MeCN as supporting electrolyte, constant potential 1.38 V (vs standard calomel reference electrode); Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Carbohydrate Chemistry, , vol. 14, # 8 p. 1217 - 1236