2,3,4,6-四-o-乙酰基-alpha-d-吡喃葡萄糖苷甲酯合成路线 （共 100 条）
参考文献
Chemische Berichte, , vol. 90, p. 2094
反应条件
hydrogen fluoride T=0°C; 2 h;
参考文献
Bergamaschi, Brian A.; Hedges, John I.
Carbohydrate Research, 1996 , vol. 280, # 2 p. 345 - 350
反应条件
rabbit serum (esterase) in various solvent(s) T=37°C; 3 h;
参考文献
Tetrahedron, , vol. 49, # 47 p. 10977 - 10986
反应条件
1: 77 percent / citrate phosphate buffer (pH 5.0), esterase from Rhodosporidium toruloides / 16 h / 30 °C 2: 63 percent / AcOH / toluene / 16 h / 80 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 6 p. 1069 - 1080
反应条件
1: NaOMe / methanol / Ambient temperature 2: pyridine / Ambient temperature View Scheme
参考文献
Raadt, Anna de; Griengl, Herfried; Klempier, Norbert; Stuetz, Arnold E.
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3179 - 3184
反应条件
1: NaOMe / methanol / Ambient temperature 2: pyridine / Ambient temperature 3: pyridine / Ambient temperature View Scheme
参考文献
Raadt, Anna de; Griengl, Herfried; Klempier, Norbert; Stuetz, Arnold E.
Journal of Organic Chemistry, 1993 , vol. 58, # 11 p. 3179 - 3184
反应条件
IRA-400(OH) resin in methanol 4 h;
参考文献
Pathak
Synthetic Communications, 1993 , vol. 23, # 1 p. 83 - 85
反应条件
tri-n-butyltin methoxide in methanol T=55°C; Rate constant;
参考文献
Herzig, Jacob; Nudelman, Abraham; Gottlieb, Hugo E.
Carbohydrate Research, 1988 , vol. 177, p. 21 - 28
反应条件
1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C 2.1: methanol; sodium methylate / 20 °C 3.1: sodium hydride / N,N-dimethyl-formamide; paraffin / 0 °C 3.2: 0 - 20 °C 4.1: N-bromosuccinmide; water / acetone / -45 - 20 °C View Scheme
参考文献
Boettcher, Stephan; Matwiejuk, Martin; Thiem, Joachim
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 413 - 420
参考文献
Bredereck et al.
Chemische Berichte, 1958 , vol. 91, p. 515,522, 524
