2-(3,5-二甲基-吡唑-1-基)-苯胺合成路线 （共 32 条）
反应条件
in ethanol T=21.85°C; 0.133333 h; Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 121, # 13 p. 3104 - 3113
反应条件
1: 86 percent / anhydrous potassium fluoride / 12 h / 120 - 140 °C 2: 5 percent / triethyl phosphite / various solvent(s) / 72 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
反应条件
hydrogen; palladium on activated charcoal in ethanol Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 581 - 585
反应条件
1: 97 percent / fuming nitric acid, 98percent sulphuric acid / 1 h / 30 °C 2: 76 percent / urea, hydrazine hydrate / ethanol 3: 74 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating 4: 97 percent / hydrogen / Raney nickel / ethanol 5: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h 6: 83.5 percent / bis-(2-methoxy-ethyl) ether / 162 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
反应条件
1: 76 percent / urea, hydrazine hydrate / ethanol 2: 74 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating 3: 97 percent / hydrogen / Raney nickel / ethanol 4: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h 5: 83.5 percent / bis-(2-methoxy-ethyl) ether / 162 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
反应条件
1: 97 percent / hydrogen / Raney nickel / ethanol 2: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h 3: 83.5 percent / bis-(2-methoxy-ethyl) ether / 162 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
反应条件
1: 74 percent / 98percent sulphuric acid / ethanol; acetic acid / 6 h / Heating 2: 97 percent / hydrogen / Raney nickel / ethanol 3: 1.) sodium nitrite, conc. hydrochloric acid, 2.) sodium azide, sodium acetate / 1.) water, 0 deg C, 2.) 1 h 4: 83.5 percent / bis-(2-methoxy-ethyl) ether / 162 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
反应条件
in cyclohexane T=20°C; 0.5 h; Irradiation;
参考文献
Chemistry Letters, , p. 331 - 334
反应条件
in benzene 3.5 h; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 113, # 18 p. 6928 - 6934
反应条件
triethyl phosphite in various solvent(s) 72 h; Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 982 - 994
