N-甲酰基-2-甲基丙氨酸合成路线 （共 4 条）
反应条件
acetic anhydride in formic acid; (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
Interx Research Corporation
Patent: US3966796 A1, 1976 ;
反应条件
1: T=20 - 55°C;
2: With acetic anhydride
T=20 - 55°C; 2 h;
3: With water
HeatingReduced pressure;
参考文献
Rotstein, Benjamin H.; Winternheimer, David J.; Yin, Lois M.; Deber, Charles M.; Yudin, Andrei K.
Chemical Communications, 2012 , vol. 48, # 31 p. 3775 - 3777
参考文献
Kjaer
Acta Chemica Scandinavica (1947-1973), 1953 , vol. 7, p. 889,896
反应条件
1: 98 percent / ethanol; diethyl ether
2: 64 percent / Et3N, diphosgen / CH2Cl2 / 1.) -10 deg C, 30 min, 2.) r.t., 1 h
View Scheme
参考文献
Hemantha, Hosahalli P.; Sureshbabu, Vommina V.
Journal of Peptide Science, 2010 , vol. 16, # 11 p. 644 - 651
