甲基3,5-二甲氧基-4-甲基苯甲酸酯合成路线 （共 25 条）
反应条件
hydrogenchloride hydrolyze;
参考文献
Manchand, Percy S.; Townsend, John M.; Belica, Peter S.; Wong, Harry S.
Synthesis, 1980 , # 5 p. 409 - 410
反应条件
bromine in tetrachloromethane Bromination; Irradiation;
参考文献
Mizutani, Tadashi; Wada, Kenji; Kitagawa, Susumu
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 6097 - 6106
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Heating;
参考文献
Elix, John A.; Jayanthi, Vilas K.
Australian Journal of Chemistry, 1987 , vol. 40, # 11 p. 1841 - 1850
反应条件
potassium carbonate in acetone
T=40°C;
参考文献
Shanghai Institute of Materia Medica, Chinese Academy of Sciences
Patent: EP2199295 A1, 2010 ;
Location in patent: Page/Page column 17 ;
反应条件
potassium carbonate in acetone
18 h; Heating;
参考文献
Cutler, Horace G.; Majetich, George; Tian, Xinrong; Spearing, Paul
Journal of Agricultural and Food Chemistry, 1997 , vol. 45, # 4 p. 1422 - 1429
反应条件
tetra-(n-butyl)ammonium iodide; potassium carbonate in acetone
Methylation; 24 h; Heating;
参考文献
Pearson, Anthony J.; Heo, Jung-Nyoung
Organic Letters, 2000 , vol. 2, # 19 p. 2987 - 2990
参考文献
Spirogen Limited
Patent: US2003/120069 A1, 2003 ;
反应条件
potassium carbonate in acetone
T=23°C; 24 h;
参考文献
Achenbach; Muhlenfeld; Brillinger
1985 , vol. 1985, # 8 p. 1596 - 1628
反应条件
1: 80 percent / p-TsOH*H2O / 24 h / Heating
2: 33 percent / K2CO3; n-Bu4NI / acetone / 24 h / Heating
View Scheme
参考文献
Pearson, Anthony J.; Heo, Jung-Nyoung
Organic Letters, 2000 , vol. 2, # 19 p. 2987 - 2990
反应条件
sulfuric acid
5 h; Heating / reflux;
参考文献
Spirogen Limited
Patent: EP1193270 A2, 2002 ;
Location in patent: Page 78, 127 ;
