1: hexadecan-1-ol With diisobutylaluminium hydride in hexane; dichloromethane
1 h; Cooling with ice;
2: (S)-(-)-glycidol in hexane; dichloromethane
T=20°C; 72 h;
3: With water; Sodium potassium tartrate in hexane; dichloromethane
0.5 h;
参考文献
North, E. Jeffrey; Osborne, Daniel A.; Bridson, Peter K.; Baker, Daniel L.; Parrill, Abby L.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 9 p. 3433 - 3442