反应条件
1: 1.) sodium salt of N-hydroxypyridine-2(1H)-thione, DMAP, 2.) tert-butylmercaptan, AIBN / 1.) benzene, reflux, 1 h, 2.) benzene, reflux, 2 h
2: NaOH / methanol / 4 h / Heating
3: SOCl2 / 0.25 h / Heating
View Scheme
参考文献
Hasegawa; Nigo; Kakita; Toyoda; Toya; Ueda
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 10 p. 1760 - 1768
