aniline in ethanol
excess of ligand was added to ethanolic suspn. of iron(II) oxalate, shaking for 5-6 h, mixt. was allowed to stand for another 6 h; filtered, washed with dry ether and finally dried in vac. desiccator over CaCl2, elem. anal.;
参考文献
Bajpai; Shukla
Journal of the Indian Chemical Society, 1980 , vol. 57, # 2 p. 219 - 221
in ethanol
excess of ligand was added to ethanolic suspn. of iron(II) oxalate, shaking for 5-6 h, mixt. was allowed to stand for another 6 h; filtered, washed with dry ether and finally dried in vac. desiccator over CaCl2, elem. anal.;
参考文献
Bajpai; Shukla
Journal of the Indian Chemical Society, 1980 , vol. 57, # 2 p. 219 - 221
ethylenediamine in ethanol
excess of ligand was added to ethanolic suspn. of iron(II) oxalate, shaking for 5-6 h, mixt. was allowed to stand for another 6 h; filtered, washed with dry ether and finally dried in vac. desiccator over CaCl2, elem. anal.;
参考文献
Bajpai; Shukla
Journal of the Indian Chemical Society, 1980 , vol. 57, # 2 p. 219 - 221
NH3 in ethanol
excess of ligand was added to ethanolic suspn. of iron(II) oxalate, shaking for 5-6 h; addn. of acetone, filtered, washed with dry ether and finally dried in vac. desiccator over CaCl2, elem. anal.;
参考文献
Bajpai; Shukla
Journal of the Indian Chemical Society, 1980 , vol. 57, # 2 p. 219 - 221
in neat (no solvent)
heating FeC2O4*2H2O in stream of N2 at 200°C, treatment with mixt. of C5H6 and CO at 380°C;;
参考文献
Gmelin Handbook: Fe: Org.Verb.A1, 2.1.1.1, page 15 - 16
Full Text Show Details
Holzapfel, H.; Huebner, H.; Geissler, C.; Rolle, W.
Patent: DE43979 , 1965 ;
C. A., 1966 , vol. 64, p. 17642
