(苯甲酰基甲基)三苯基溴化膦合成路线 （共 33 条）
反应条件
1: 90 percent / aq. NaOH / methanol / 20 °C
2: 56 percent / benzene / Heating
3: 52 percent / NaOMe / methanol / 20 °C
View Scheme
参考文献
Babu, K. Suresh; Li, Xing-Cong; Jacob, Melissa R.; Zhang, Qifeng; Khan, Shabana I.; Ferreira, Daneel; Clark, Alice M.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7877 - 7886
反应条件
sodium hydroxide in solid
thorough grounding a mixt. of aldehyde and phosphonium salt with NaOH atroom temp., heating at 65°C for 240 min, grounding for 1-2 min, cooling to room temp.; extn. with CH2Cl2, drying with Na2SO4, filtration, evapn., chromy (SiO2,petroleum ether);
参考文献
Liu, Wan-Yi; Xu, Qi-Hai; Ma, Yong-Xiang; Liang, Yong-Min; Dong, Ning-Li; Guan, De-Peng
Journal of Organometallic Chemistry, 2001 , vol. 625, # 1 p. 128 - 131
反应条件
1: sodium hydroxide / water
2: 226.84 °C / Pyrolysis
View Scheme
参考文献
Al-Bashir, Rasha F.; Al-Awadi, Nouria A.; El-Dusouqui, Osman M. E.
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 4 p. 311 - 319
