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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-苯基萘
合成路线
（共 341 条）
108-86-1
溴代苯
+
630-95-5
alpha,alpha-二苯基萘-1-甲醇
→
反应条件
605-02-7
1-苯基萘
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 8 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
6301-54-8
2-萘-1-基丙-2-醇
+
108-90-7
氯苯
→
反应条件
605-02-7
1-苯基萘
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 22 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
630-95-5
alpha,alpha-二苯基萘-1-甲醇
+
108-90-7
氯苯
→
反应条件
605-02-7
1-苯基萘
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 4 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
→
反应条件
605-02-7
1-苯基萘
+
1357920-87-6
+
1182708-58-2
反应条件
[Ru(tetraphenylporphyrin(-2H))(3,5-(CF3)2C6H3N)2 in benzene 1.5 h; RefluxInert atmosphere;
参考文献
Chemical Communications, , # 26 p. 3952 - 3954
76-86-8
三苯基氯硅烷
+
90-11-9
1-溴代萘
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=100°C; 5 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
1048-08-4
四苯基硅烷
+
90-14-2
1-碘萘
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=100°C; 16 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
90-11-9
1-溴代萘
+
22702-76-7
氯(二甲基)苯基锗烷
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=100°C; 15 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 23 p. 8199 - 8212
90-11-9
1-溴代萘
+
80-10-4
二苯二氯硅烷
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; water in tetrahydrofuran; toluene T=115°C; 5 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
90-14-2
1-碘萘
+
595-90-4
四苯基锡
→
反应条件
604-53-5
1,1'-联萘
+
605-02-7
1-苯基萘
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
90-15-3
1-萘酚
+
98-80-6
→
反应条件
92-52-4
+
605-02-7
1-苯基萘
反应条件
1: α-naphthol With potassium phosphate; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: 3,4,5-trimethoxyphenylboronic acid With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Huang, Jie; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2011 , vol. 17, # 14 p. 4038 - 4042
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