2,3-吡啶二甲酸二甲酯合成路线 （共 24 条）
反应条件
1: 85 percent / NaBH4 / ethanol / 17 h / Heating
2: 26 percent / SOCl2 / CH2Cl2 / 1 h / 75 °C
View Scheme
参考文献
Sperry, Jeffrey B.; Farr, Roger M.; Levent, Mahmut; Ghosh, Mousumi; Hoagland, Steven M.; Varsolona, Richard J.; Sutherland, Karen
Organic Process Research and Development, 2012 , vol. 16, # 11 p. 1854 - 1860
反应条件
1: sodium tetrahydroborate
2: selenium(IV) oxide / 1,4-dioxane / 4 h / |Reflux
View Scheme
参考文献
Niaz, Basit; Iftikhar, Fatima; Kindermann, Markus K.; Jones, Peter G.; Heinicke, Joachim
European Journal of Inorganic Chemistry, 2013 , # 24 p. 4220 - 4227
反应条件
sodium tetrahydroborate in ethanol
T=0°C; Reflux;
参考文献
Tang, Yan Bo; Zhang, Qing Jian; Yu, De Quan
Chinese Chemical Letters, 2012 , vol. 23, # 10 p. 1122 - 1124
反应条件
1: potassium tert-butylate / toluene; tetrahydrofuran / 2 h / 55 - 60 °C
2: hydrogenchloride / water / 5 h / 75 - 80 °C
View Scheme
参考文献
Leahy, David K.; Fan, Yu; Desai, Lopa V.; Chan, Collin; Zhu, Jason; Hanson, Ronald L.; Sugiyama, Masano; Rosner, Thorsten; Cuniere, Nicolas; Guo, Zhiwei; Hsiao, Yi; Luo, Guanglin; Chen, Ling; Gao, Qi
Organic Letters, 2012 , vol. 14, # 18 p. 4938 - 4941,4
