1: Et3N / CHCl3 / 0.58 h 2: trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Kondo, Hiroki; Takaki, Katsunori; Kuroki, Ryoichi; Tada, Akihiro; Fukumoto, Kunihiro; Sunamoto, Junzo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 2957 - 2961
sodium hydrogencarbonate in water; acetone T=20°C; Substitution; pH=9.5; 1 h;
参考文献
LeFevre, Joseph W.; Bonzagni, Neil J.; Chappell, Lara L.; Clement, David J.; Albro, Jeb R.; Lezynski, Denise M.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 6 p. 477 - 489
1: C72H110N12O20 With hydrogenchloride; water T=110°C; 12 h; 2: 5-dimethylamino-1-naphthalenesulfonyl chloride With sodium hydrogencarbonate in acetone T=20°C; 14 h;