(3,3,3-三氯丙-1-烯基)苯合成路线 (共 6 条)
反应条件
T=35 - 40°C; 38 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
in cyclohexane
T=65°C; 18 h; Further byproducts given;
参考文献
Jiang, Xi-Kui; Ji, Guo-Zhen; Xie, John Rong-Yuan
Tetrahedron, 1996 , vol. 52, # 8 p. 3017 - 3028
参考文献
Kharasch; Reinmuth; Urry
Journal of the American Chemical Society, 1947 , vol. 69, p. 1108
Full Text Show Details
U.S. Rubber Co.
Patent: US2468208 , 1946 ;
反应条件
in cyclohexane
T=65°C; 18 h; other p-substituted phenylacetylenes, relative rates of trichloromethyl-bromo-addition; Mechanism;
参考文献
Jiang, Xi-Kui; Ji, Guo-Zhen; Xie, John Rong-Yuan
Tetrahedron, 1996 , vol. 52, # 8 p. 3017 - 3028
参考文献
Kharasch; Reinmuth; Urry
Journal of the American Chemical Society, 1947 , vol. 69, p. 1108
Full Text Show Details
U.S. Rubber Co.
Patent: US2468208 , 1946 ;
反应条件
1: SbF3 / dioxane
2: Br2 / CHCl3 / Irradiation
3: Et3N
4: KOH / 250 °C
View Scheme
参考文献
Yagupol'skii,L.M.; Fialkov,Yu.A.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 1291 - 1294,1318 - 1321