2,5-二甲基-1,4-苯二甲酸合成路线 （共 27 条）
反应条件
vanadium pentoxide T=400°C; effect of temperature on gas-phase oxidation; Product distribution;
参考文献
Sharipov, A. Kh.; Masagutov, R. M.; Rafikov, S. R.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 4 p. 817 - 820
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 4 p. 925 - 928
反应条件
vanadium pentoxide T=400°C; effect of temperature on gas-phase oxidation; Product distribution;
参考文献
Sharipov, A. Kh.; Masagutov, R. M.; Rafikov, S. R.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 4 p. 817 - 820
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 4 p. 925 - 928
反应条件
1: PCl5 2: aluminium chloride View Scheme
参考文献
de Diesbach
Helvetica Chimica Acta, 1923 , vol. 6, p. 546
反应条件
1: in methanol; hexanes; diethyl ether
T=0 - 20°C; 0.5 h;
2: With acetic acid in methanol; hexanes; diethyl ether
参考文献
EXELIXIS, INC.
Patent: WO2009/55077 A1, 2009 ;
Location in patent: Page/Page column 404-405 ;
反应条件
thionyl chloride
3 h; Heating / reflux;
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: EP1403255 A1, 2004 ;
Location in patent: Page 129 ;
EP 1403255 A1
反应条件
1: MeSO3H / 10 h / Heating
2: 42 percent / NBS, benzoyl peroxide / CCl4 / 21 h / Heating
View Scheme
参考文献
Ngola, Sarah M.; Kearney, Patrick C.; Mecozzi, Sandro; Russell, Keith; Dougherty, Dennis A.
Journal of the American Chemical Society, 1999 , vol. 121, # 6 p. 1192 - 1201
反应条件
1: PCl5
2: aluminium chloride
View Scheme
参考文献
de Diesbach
Helvetica Chimica Acta, 1923 , vol. 6, p. 546
