1,2-二癸酰基-sn-甘油合成路线 （共 7 条）
反应条件
Fusarium solani lipase in aq. buffer T=25°C; pH=8; Enzymatic reaction; KineticsCatalytic behavior; Concentration; regioselective reaction;
参考文献
Jallouli, Raida; Fendri, Ahmed; Mechichi, Tahar; Gargouri, Youssef Talel; Bezzine, Sofiane
Chirality, 2013 , vol. 25, # 1 p. 35 - 38
反应条件
hydrogen; acetic acid; palladium on activated charcoal in ethanol; ethyl acetate
P=2068.59 Torr; 18 h;
参考文献
Ali, Shoukath M.; Ahmad, Moghis U.; Koslosky, Peter; Kasireddy, Krishnudu; Murali Krishna; Ahmad, Imran
Tetrahedron, 2006 , vol. 62, # 29 p. 6990 - 6997
反应条件
Rhizomucor miehei 1,3-specific lipase immobilized by adsorption on anion exchange phenolic resin Duolite A-568; silica gel in n-heptane
T=40°C; 6 h; Enzymatic reaction;
参考文献
Sanchez, Daniel Alberto; Tonetto, Gabriela Marta; Ferreira, Maria Lujan
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 7 - 18
反应条件
Rhizomucor miehei 1,3-specific lipase immobilized by adsorption on anion exchange phenolic resin Duolite A-568; silica gel in n-heptane
T=50°C; 6 h; Enzymatic reaction; ConcentrationTemperature;
参考文献
Sanchez, Daniel Alberto; Tonetto, Gabriela Marta; Ferreira, Maria Lujan
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 100, p. 7 - 18
反应条件
1: 32 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2 / 12 h / 20 °C
2: 94 percent / hydrogen; acetic acid / Pd-C / ethanol; ethyl acetate / 18 h / 2068.59 Torr
View Scheme
参考文献
Ali, Shoukath M.; Ahmad, Moghis U.; Koslosky, Peter; Kasireddy, Krishnudu; Murali Krishna; Ahmad, Imran
Tetrahedron, 2006 , vol. 62, # 29 p. 6990 - 6997
反应条件
1: DMAP; DCC / diethyl ether
2: H2 / Pd/C / methanol
View Scheme
参考文献
Marguet, Frank; Cavalier, Jean-Francois; Verger, Robert; Buono, Gerard
European Journal of Organic Chemistry, 1999 , # 7 p. 1671 - 1678
反应条件
Tris-HCl buffer
T=37°C; pH=7.4; Enzyme kinetics;
参考文献
Liu, Yan; Ogawa, Katsu; Schanze, Kirk S.
Analytical Chemistry, 2008 , vol. 80, # 1 p. 150 - 158
