2-氯-5-硝基-3-吡啶羧酰胺合成路线 （共 11 条）
反应条件
ammonia in water; acetonitrile T=-20 - 0°C; 0.25 h;
参考文献
Ryabova; Makarov; Alekseeva; Shashhov; Chernyshev; Granik
Russian Chemical Bulletin, 2005 , vol. 54, # 8 p. 1907 - 1914
反应条件
1: nitric acid; sulfuric acid / 1 h / 20 °C 2: thionyl chloride / CCl4 3: 64 percent / ammonia / acetonitrile; H2O / 0.25 h / -20 - 0 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 54, # 8 p. 1907 - 1914
反应条件
1: thionyl chloride / CCl4 2: 64 percent / ammonia / acetonitrile; H2O / 0.25 h / -20 - 0 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 54, # 8 p. 1907 - 1914
反应条件
1: thionyl chloride / 3 h / Reflux 2: ammonia / water; acetone / 0.17 h / 25 °C View Scheme
反应条件
1.1: nitric acid; sulfuric acid / 18 h / 0 - 30 °C 1.2: 1 h / 100 °C 2.1: trichlorophosphate / 8 h / Reflux 3.1: sodium dichromate; sulfuric acid / 15 h / 30 °C 4.1: thionyl chloride / 3 h / Reflux 5.1: ammonia / water; acetone / 0.17 h / 25 °C View Scheme
反应条件
1: trichlorophosphate / 8 h / Reflux 2: sodium dichromate; sulfuric acid / 15 h / 30 °C 3: thionyl chloride / 3 h / Reflux 4: ammonia / water; acetone / 0.17 h / 25 °C View Scheme
反应条件
1: sodium dichromate; sulfuric acid / 15 h / 30 °C 2: thionyl chloride / 3 h / Reflux 3: ammonia / water; acetone / 0.17 h / 25 °C View Scheme
反应条件
1: nitric acid; sulfuric acid 2: thionyl chloride / |Reflux 3: ammonia / water View Scheme
参考文献
Antimicrobial Agents and Chemotherapy, , vol. 58, # 1 p. 55 - 60
反应条件
1: thionyl chloride / |Reflux 2: ammonia / water View Scheme
参考文献
Antimicrobial Agents and Chemotherapy, , vol. 58, # 1 p. 55 - 60
反应条件
thionyl chloride Reflux;
参考文献
Salina, Elena; Ryabova, Olga; Kaprelyants, Arseny; Makarov, Vadim
Antimicrobial Agents and Chemotherapy, 2014 , vol. 58, # 1 p. 55 - 60
