6-溴苯并[d][1,3]二氧代-5-羧酸合成路线 （共 26 条）
反应条件
2: 75 percent / Pd0/Na2CO3 / 1,2-dimethoxy-ethane / Heating 4: 2,6-lutidine / 0.5 h / Ambient temperature 5: TBAF, H2O / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Siddiqui, M.A.; Snieckus, V.
Tetrahedron Letters, 1988 , vol. 29, # 43 p. 5463 - 5466
反应条件
sodium chlorite; phosphoric acid; dihydrogen peroxide in water; acetone
Ambient temperature;
参考文献
Padwa, Albert; Dimitroff, Martin; Waterson, Alex G.; Wu, Tianhua
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 3986 - 3997
反应条件
sodium methylate in dimethyl sulfoxide
T=150°C; 0.0194444 h;
参考文献
Kobayashi, Shigeru; Imakura, Yasuhiro; Horikawa, Ritsuko
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 4 p. 1287 - 1293
参考文献
Fales et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5885,5889
反应条件
1: NBS / CH2Cl2
2: PCC / CH2Cl2
3: CrO3; H2SO4 / acetone
View Scheme
参考文献
Bressy, Cyril; Menant, Christine; Piva, Olivier
Synlett, 2005 , # 4 art. no. D35104ST, p. 577 - 582
反应条件
1: PCC / CH2Cl2
2: CrO3; H2SO4 / acetone
View Scheme
参考文献
Bressy, Cyril; Menant, Christine; Piva, Olivier
Synlett, 2005 , # 4 art. no. D35104ST, p. 577 - 582
反应条件
in dimethyl sulfoxide
T=150°C; 0.0194444 h;
参考文献
Kobayashi, Shigeru; Imakura, Yasuhiro; Horikawa, Ritsuko
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 4 p. 1287 - 1293
反应条件
N-bromosuccinmide
T=110°C;
参考文献
Yamaguchi
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 513
Chem.Abstr., 1958 , p. 9014
反应条件
1: Br2; AcONa; AcOH
2: Jones reagent
View Scheme
参考文献
Rys, Veronique; Couture, Axel; Deniau, Eric; Lebrun, Stephane; Grandclaudon, Pierre
Tetrahedron, 2005 , vol. 61, # 3 p. 665 - 671
反应条件
N-bromosuccinmide; chloroform
Behandeln der Reaktionsloesung mit Ammoniak;
参考文献
Yamaguchi
Nippon Kagaku Kaishi, 1956 , vol. 77, p. 591,592
Chem.Abstr., 1958 , p. 305
