4-(2-甲基-1,3-二氧戊环-2-基)吡啶合成路线 (共 5 条)
反应条件
tetra(n-butyl)ammonium dichromate(VI) 0.0333333 h; microwave irradiation;
参考文献
Chemistry Letters, , vol. 33, # 8 p. 1038 - 1039
反应条件
1: 1-(pyridin-4-yl)ethanone With hydrogenchloride in toluene
2: ethylene glycol With toluene-4-sulfonic acid in toluene
3 h; Heating;
参考文献
Beach, J. Warren; Damaj, M. Imad; Jonnala, Ramamohana R.; Terry Jr., Alvin V.; Buccafusco, Jerry J.
Medicinal Chemistry Research, 1998 , vol. 8, # 9 p. 510 - 522
反应条件
toluene-4-sulfonic acid in toluene
3 h; Heating;
参考文献
Beach, J. Warren
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1861 - 1863
反应条件
1: acetone / Heating
2: NaBH4 / ethanol / 1 h / 0 - 5 °C
View Scheme
参考文献
Besselievre; Husson
Tetrahedron Letters, 1976 , vol. No. 22, p. 1873 - 1876
反应条件
in acetonitrile
Heating;
参考文献
Beach, J. Warren; Damaj, M. Imad; Jonnala, Ramamohana R.; Terry Jr., Alvin V.; Buccafusco, Jerry J.
Medicinal Chemistry Research, 1998 , vol. 8, # 9 p. 510 - 522