2-(2-甲氧基苯基)乙酸乙酯合成路线 (共 13 条)
反应条件
pyridinium p-toluenesulfonate; lithium diisopropyl amide 1.) THF, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Oda, Mitsunori; Kamata, Yoshitaka; Nishii, Satoshi; Miyatake, Ryuta; Kuroda, Shigeyasu; Oda, Masaji
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 10 p. 445 - 446
反应条件
bis(η3-allyl-μ-chloropalladium(II)); dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,3,5-trimethyl-benzene
T=20 - 140°C; 36.1667 h; Inert atmosphereSealed tube;
参考文献
Shang, Rui; Ji, Dong-Sheng; Chu, Ling; Fu, Yao; Liu, Lei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 19 p. 4470 - 4474
反应条件
4-(N,N-dimethlyamino)pyridine; bis(η3-allyl-μ-chloropalladium(II)); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,3,5-trimethyl-benzene
T=140°C; 20 h; Inert atmosphere;
参考文献
Feng, Yi-Si; Wu, Wei; Xu, Zhong-Qiu; Li, Yan; Li, Ming; Xu, Hua-Jian
Tetrahedron, 2012 , vol. 68, # 9 p. 2113 - 2120
反应条件
zinc dibromide; bis (triortho-tolylphosphine)palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; 5 h;
参考文献
Kosugi, Masanori; Negishi, Yoshikazu; Kameyama, Masayuki; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 11 p. 3383 - 3384
反应条件
sulfuric acid in chloroform
10 h; Heating;
参考文献
Cordes, Jens; Harms, Klaus; Koert, Ulrich
Organic Letters, 2010 , vol. 12, # 17 p. 3808 - 3811
反应条件
potassium carbonate; copper(I) oxide; tetrakis(triphenylphosphine) palladium(0)
T=80°C;
参考文献
Liu, Xing-Xin; Deng, Min-Zhi
Chemical Communications, 2002 , # 6 p. 622 - 623
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,3-bis-(diphenylphosphino)propane; palladium diacetate in 1-methyl-pyrrolidin-2-one
T=150°C; 16 h; Inert atmosphere;
参考文献
Gruenberg, Matthias F.; Goossen, Lukas J.
Chemistry - A European Journal, 2013 , vol. 19, # 23 p. 7334 - 7337
反应条件
potassium phosphate; copper(l) iodide; ethanol in dimethyl sulfoxide
T=80°C; 20 h; Inert atmosphere;
参考文献
Ke, Jie; He, Chuan; Liu, Huiying; Xu, Huan; Lei, Aiwen
Chemical Communications, 2013 , vol. 49, # 60 p. 6767 - 6769
反应条件
potassium iodide; lt;1,5-HDRhClgt;2
参考文献
Alper, Howard; Hamel, Nathalie; Smith, David J. H.; Woell, James B.
Tetrahedron Letters, 1985 , vol. 26, # 19 p. 2273 - 2274
参考文献
Rios-Lombardia, Nicolas; Busto, Eduardo; Garcia-Urdiales, Eduardo; Gotor-Fernandez, Vicente; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2571 - 2574