6-甲氧基-1,2-二氢-萘合成路线 (共 11 条)
反应条件
1: 95 percent / 10percent aq. NaHCO3, 3-chloroperbenzoic acid / toluene / 2 h / Ambient temperature 2: 74 percent / ZnI2 / benzene / 3 h / Heating View Scheme
参考文献
Hauser, Frank M.; Prasanna, Subbarao
Synthesis, 1980 , # 8 p. 621 - 623
反应条件
3,4,5,6-tetrachloro-1,2-benzoquinone in 1,2-dichloro-benzene T=25 - 52.8°C; Kinetics;
参考文献
Radtke, Rainer; Hintze, Horst; Roesler, Klaus; Heesing, Albert
Chemische Berichte, 1990 , vol. 123, p. 627 - 634
反应条件
sulfuric acid; silica gel in toluene
T=100°C; 0.5 h;
参考文献
Chavez; Suarez; Diaz
Synthetic Communications, 1994 , vol. 24, # 16 p. 2325 - 2339
反应条件
toluene-4-sulfonic acid; 2(R),4(R)-dihydroxypentane in toluene
36 h; Heating;
参考文献
Vuligonda, Vidyasagar; Lin, Yuan; Chandraratna, Roshantha A.S.
Tetrahedron Letters, 1996 , vol. 37, # 12 p. 1941 - 1944
反应条件
N-bromosuccinmide in chloroform
2 h; Heating;
参考文献
Trost,B.M.; Vladuchick,W.C.; Bridges,A.J.
Journal of the American Chemical Society, 1980 , vol. 102, p. 3554
参考文献
Medivir AB
Patent: US2003/92743 A1, 2003 ;
反应条件
zirconium tetrachloride in acetonitrile
T=20°C; 0.75 h;
参考文献
Das, Biswanath; Krishnaiah, Maddeboina; Veeranjaneyulu, Boyapati; Srinivas, Yallamalla; Rao, Yerra Koteswara
Journal of Chemical Research, 2007 , # 12 p. 717 - 719
反应条件
thionyl chloride
Title compound not separated from byproducts;
参考文献
Perrone, R; Berardi, F; Tortorella, V; Govoni, S; Lograno, MD; Daniele, E
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 9 p. 869 - 874
反应条件
1: polyphosphoric acid
2: diethyl ether / Erhitzen des Reaktionsprodukts mit NaHSO4 auf 170grad
View Scheme
参考文献
Rao; Dev
Journal of the Indian Chemical Society, 1957 , vol. 34, p. 255,261
反应条件
diethyl ether
Erhitzen des Reaktionsprodukts mit NaHSO4 auf 170grad;
参考文献
Rao; Dev
Journal of the Indian Chemical Society, 1957 , vol. 34, p. 255,261