(S)-(+)-5-(1-羟基-1-甲基乙基)-2-甲基-2-环己烯-1-酮合成路线 (共 7 条)
反应条件
in water T=210°C; 0.166667 h; Yield given. Yields of byproduct given;
参考文献
An, Jingyi; Bagnell, Laurence; Cablewski, Teresa; Strauss, Christopher R.; Trainor, Robert W.
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2505 - 2511
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol
T=65°C; 20 h;
参考文献
Mandal, Sunil K.; Jensen, David R.; Pugsley, Jacob S.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4600 - 4603
反应条件
in water
T=210°C; 0.166667 h;
参考文献
An, Jingyi; Bagnell, Laurence; Cablewski, Teresa; Strauss, Christopher R.; Trainor, Robert W.
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2505 - 2511
反应条件
manganese(IV) oxide in acetone
48 h;
参考文献
Selva, Antonio; Ferrario, Francesco; Ventura, Paolo; Pellegata, Renato
Organic Mass Spectrometry, 1987 , vol. 22, p. 523 - 529
反应条件
manganese(IV) oxide in chloroform
Ambient temperature; Yield given;
参考文献
Mori, Kenji; Igarashi, Yasuhiro
Liebigs Annalen der Chemie, 1988 , p. 93 - 96
反应条件
1: LiAlH4 / diethyl ether / 1 h / Ambient temperature
2: MnO2 / CHCl3 / Ambient temperature
View Scheme
参考文献
Mori, Kenji; Igarashi, Yasuhiro
Liebigs Annalen der Chemie, 1988 , p. 93 - 96
反应条件
Picea abies cells immobilized on alginate beads
T=24°C; Further byproducts given;
参考文献
Vanek, Tomas; Halik, Jan; Vankova, Radmila; Valterova, Irena
Bioscience, Biotechnology and Biochemistry, 2005 , vol. 69, # 2 p. 321 - 325