2,4'-二羟基二苯甲酮合成路线 （共 38 条）
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 1446,1451
反应条件
1: AlCl3 / anschliessendes Behandeln mit Eis und wss.HCl
2: KOH
View Scheme
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 1446,1451
反应条件
1: CH2Cl2 / 8 h
2: 44 percent / tetra-n-butylammonium fluoride / tetrahydrofuran; CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Cremins, Peter J.; Saengchantara, Suthiweth T.; Wallace, Timothy W.
Tetrahedron, 1987 , vol. 43, # 13 p. 3075 - 3082
反应条件
aluminium trichloride
T=20°C;
参考文献
Nussbaumer, Peter; Bilban, Melitta; Billich, Andreas
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 16 p. 2093 - 2095
反应条件
1: BuLi / tetrahydrofuran / 3 h / -70 - 20 °C
2: MnO2 / CH2Cl2 / 20 °C
3: HF / acetonitrile / 20 °C
4: aluminium chloride / 20 °C
View Scheme
参考文献
Nussbaumer, Peter; Bilban, Melitta; Billich, Andreas
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 16 p. 2093 - 2095
反应条件
1: BuLi / tetrahydrofuran / 3 h / -70 - 20 °C
2: MnO2 / CH2Cl2 / 20 °C
3: HF / acetonitrile / 20 °C
4: aluminium chloride / 20 °C
View Scheme
参考文献
Nussbaumer, Peter; Bilban, Melitta; Billich, Andreas
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 16 p. 2093 - 2095
反应条件
1: MnO2 / CH2Cl2 / 20 °C
2: HF / acetonitrile / 20 °C
3: aluminium chloride / 20 °C
View Scheme
参考文献
Nussbaumer, Peter; Bilban, Melitta; Billich, Andreas
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 16 p. 2093 - 2095
反应条件
1: HF / acetonitrile / 20 °C
2: aluminium chloride / 20 °C
View Scheme
参考文献
Nussbaumer, Peter; Bilban, Melitta; Billich, Andreas
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 16 p. 2093 - 2095
参考文献
Michael
American Chemical Journal, 1883 , vol. 5, p. 89
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1883 , p. 1120
反应条件
aluminium trichloride
参考文献
Amin; Desai
Journal of Scientific and Industrial Research, 1954 , vol. 13 B, p. 178
