2,4,6-三硝基苯甲醚合成路线 (共 124 条)
反应条件
1: 95 percent / KI / ethanol / Heating
2: 100 percent / PBr3 / toluene; dimethylformamide / Heating
View Scheme
参考文献
Bellamy, Anthony J.; Hudson, P. Nick
Tetrahedron, 1996 , vol. 52, # 15 p. 5639 - 5642
参考文献
Blanksma
Chem. Zentralbl., 1909 , vol. 80, # I p. 1809
反应条件
hydrogenchloride; tin
Kochen des Dihydrochlorids des dargestellten Oxy-methoxy-diamino-benzols mit Wasser, dem SnCl2 zugesetzt ist, unter Einleiten von Kohlendioxyd;
参考文献
Baker; Downing; Floyd; Gilbert; Ollis
Journal of the Chemical Society. Perkin transactions 1, 1970 , vol. 9, p. 1219 - 1223
反应条件
in acetonitrile-D3
T=-40 - 20°C; MeOK, Me4NOH; var. solvents and temp.; Mechanism;
参考文献
Buncel, Erwin; Dust, Julian M.; Jonczyk, Andrzej; Manderville, Richard A.; Onyido, Ikenna
Journal of the American Chemical Society, 1992 , vol. 114, # 14 p. 5610 - 5619
反应条件
potassium iodide in dimethylsulfoxide-d6
other reagents; Product distribution;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36
反应条件
potassium iodide in tetrahydrofuran
formation of intermediate σ-complex, NMR spectrum of the σ-complex; Product distributionMechanism;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36
反应条件
potassium iodide
formation of intermediate σ-complex, UV spectrum of the σ-complex; Product distributionMechanism;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36
反应条件
in tetrahydrofuran
formation of intermediate σ-complex, NMR spectrum of σ-complex, UV spectrum of σ-complex; Product distribution;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36
反应条件
potassium iodide
formation of intermediate σ-complex, UV spectrum of the σ-complex; Product distributionMechanism;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36
反应条件
potassium iodide
formation of intermediate σ-complex, UV spectrum of the σ-complex; Product distributionMechanism;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O.A.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # l p. 25 - 31
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 29 - 36