3,3-二苯基-2-丙烯酸合成路线 （共 82 条）
反应条件
titanium chloride in dichloromethane
T=-70 - 20°C; 120 h;
参考文献
Bellassoued, Moncef; Mouelhi, Sinda; Fromentin, Pierre; Gonzalez, Aurelien
Journal of Organometallic Chemistry, 2005 , vol. 690, # 9 p. 2172 - 2179
反应条件
formic acid
T=145 - 150°C; man kocht das Reaktionsprodukt mit verd. Natronlauge;
参考文献
Rupe
Justus Liebigs Annalen der Chemie, 1913 , vol. 395, p. 138
反应条件
tert.-butylhydroperoxide; acetic anhydride; p-benozquinone; palladium diacetate in acetic acid
Heating;
参考文献
Jia, Chengguo; Lu, Wenjun; Kitamura, Tsugio; Fujiwara, Yuzo
Organic Letters, 1999 , vol. 1, # 13 p. 2097 - 2100
反应条件
18-crown-6 ether in benzene
5 h; Ambient temperature;
参考文献
Frimer, Aryeh A.; Gilinsky-Sharon, Pessia; Aljadeff, Gladis; Gottlieb, Hugo E.; Hameiri-Buch, Judith; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4853 - 4866
反应条件
1: sodium amide; diethyl ether
2: P2O5; benzene
3: aq.-ethanolic KOH
View Scheme
参考文献
Lettre; Wick
Justus Liebigs Annalen der Chemie, 1957 , vol. 603, p. 189,196
反应条件
tert.-butylhydroperoxide; acetic anhydride; p-benozquinone; palladium diacetate in acetic acid
Heating;
参考文献
Jia, Chengguo; Lu, Wenjun; Kitamura, Tsugio; Fujiwara, Yuzo
Organic Letters, 1999 , vol. 1, # 13 p. 2097 - 2100
反应条件
phosphorus pentoxide
参考文献
Blicke; Faust
Journal of the American Chemical Society, 1954 , vol. 76, p. 3159
反应条件
1: 56 percent / t-butyl perbenzoate / Pd(OCOPh)2 / acetic acid / 3 h / 100 °C
View Scheme
参考文献
Tsuji, Jiro; Nagashima, Hideo
Tetrahedron, 1984 , vol. 40, # 14 p. 2699 - 2702
反应条件
1: t-butyl perbenzoate / Pd(OCOPh)2 / acetic acid / 3 h / 100 °C
2: 56 percent / t-butyl perbenzoate / Pd(OCOPh)2 / acetic acid / 3 h / 100 °C
View Scheme
参考文献
Tsuji, Jiro; Nagashima, Hideo
Tetrahedron, 1984 , vol. 40, # 14 p. 2699 - 2702
参考文献
Hennion; Fleck
Journal of the American Chemical Society, 1955 , vol. 77, p. 3253,3257
