1,3,3-三苯基-1-丙酮合成路线 (共 136 条)
反应条件
formic acid; polystyrene-bound IrCl(CO)(PPh3)2 in toluene
T=97°C; 8 h;
参考文献
Azran, Jacques; Buchman, Ouri; Orchin, Milton; Blum, Jochanan
Journal of Organic Chemistry, 1984 , vol. 49, p. 1327 - 1333
反应条件
1: Poly(phenylmethylsiloxane) With potassium carbonate in toluene
T=20°C; 1 h;
2: trans-1,3-diphenyl-2-propen-1-one With water; [Rh(OH)(cycloocta-1,5-diene)]2 in toluene
T=120°C; 24 h;
参考文献
Koike, Tooru; Du, Xiaoli; Mori, Atsunori; Osakada, Kohtaro
Synlett, 2002 , # 2 p. 301 - 303
反应条件
in tetrahydrofuran
T=0°C; 30 h;
参考文献
Imamoto, Tsuneo; Takiyama, Noboyuki; Nakamura, Kimikazu; Hatajima, Toshihiko; Kamiya, Yasuo
Journal of the American Chemical Society, 1989 , vol. 111, # 12 p. 4392 - 4398
反应条件
trifluorormethanesulfonic acid; SbF5
T=23°C; 8 h;
参考文献
Ohwada, Tomohiko; Yamagata, Naoko; Shudo, Koichi
Journal of the American Chemical Society, 1991 , vol. 113, # 4 p. 1364 - 1373
反应条件
Cu(BF4)2; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane; water
T=75°C; 23 h;
参考文献
Nishikata, Takashi; Yamamoto, Yasunori; Miyaura, Norio
Chemistry Letters, 2003 , vol. 32, # 8 p. 752 - 753
反应条件
bis(acetylacetonato) palladium; oxygen in 1,4-dioxane; water
T=80°C; P=760.051 Torr; 24 - 32 h;
参考文献
Chen, Wen; Chen, Hui; Xiao, Fuhong; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 26 p. 4295 - 4298
反应条件
formic acid; triethylamine; [Pd(PPh3)2(OAc)2] in acetonitrile
T=80°C; 7 h; Yields of byproduct given;
参考文献
Cacchi, S.; Arcadi, A.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4236 - 4240
反应条件
trifluorormethanesulfonic acid
T=23°C; 24 h;
参考文献
Ohwada, Tomohiko; Yamagata, Naoko; Shudo, Koichi
Journal of the American Chemical Society, 1991 , vol. 113, # 4 p. 1364 - 1373
反应条件
lithium chloride; palladium dichloride in acetic acid
T=50°C; Addition; Michael reaction; 2 h;
参考文献
Ohe; Wakita; Motofusa; Cho; Uemura
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 9 p. 2149 - 2155
反应条件
indium(III) chloride in tetrahydrofuran
T=0 - 20°C; 16 h;
参考文献
Kelly, Brian G.; Gilheany, Declan G.
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 887 - 890