iodine
1.) THF, RT, 2.) a) -78 deg C, 3 h, b) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rieke, Reuben D.; Schulte, Louis D.; Dawson, Bryan T.; Yang, Sheng Sbeng
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8388 - 8398
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853
potassium-sodium
1.) glyme, triglyme, 0 deg C, 3 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Collins, Clair J.; Hombach, Hans-Peter; Maxwell, Brian; Woody, Madge C.; Benjamin, Ben M.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 851 - 853