反应条件
1: carbon dioxide; AlMe2(OMe); 2-(furan-2-yl)-pyridine With [(η2-cyclooctene)4Rh2(μ-Cl)2]; tri-cyclo-hexyl-phosphine in methanol; N,N-dimethyl acetamide
T=70°C; P=760.051 Torr; 8 h; Inert atmosphere;
2: diazomethyl-trimethyl-silane in methanol; diethyl ether
T=0°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Mizuno, Hajime; Takaya, Jun; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2011 , vol. 133, # 5 p. 1251 - 1253
