二(三叔丁基膦)铂(0)合成路线 (共 14 条)
反应条件
sodium methylate in methanol soln. of Pt complex in benzene was added to MeOH soln. of MeONe; stirring for 5 h; evapn., extn. with pentane, evapn.;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824
反应条件
potassium hydroxide in ethanol; benzene soln. of Pt complex in benzene was treated with EtOH soln. of KOH; react. time 1 h; evapn., recrystn.;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824
反应条件
ethanol in ethanol byproducts: H2; room temp., ca 3 weeks;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824
反应条件
ammonia in acetone under Ar; bubbling of NH3 through an acetone solution of the Pt complex at 25°C; filtration, washing with acetone, drying, NMR anal.;
参考文献
Goel, Ram G.; Srivastava, Ramesh C.
Journal of Organometallic Chemistry, 1983 , vol. 244, # 3 p. 303 - 310
反应条件
ammonia in acetone under Ar; bubbling of NH3 through an acetone solution of the Pt complex at 25°C; filtration, washing with acetone, drying, NMR anal.;
参考文献
Goel, Ram G.; Srivastava, Ramesh C.
Journal of Organometallic Chemistry, 1983 , vol. 244, # 3 p. 303 - 310
反应条件
sodium tetrahydroborate in ethanol NaBH4 was added to stirred soln. of Pt complex; stirring for 30 min; evapn., extn. with pentane, evapn., recrystn. from hexane; elem. anal.;
参考文献
Organometallics, , vol. 1, p. 819 - 824
反应条件
potassium hydroxide in ethanol under argon, at 35-40°C, for 48 h; evapd. in vac., residue extd. with hexane, ext. concd. and cooled, crystn.; elem. anal.;
参考文献
Goel, Ram G.; Ogini, William O.; Srivastava, Ramesh C.
Journal of Organometallic Chemistry, 1981 , vol. 214, # 3 p. 405 - 417
反应条件
KOH or NaOMe in benzene alcoholic soln. of KOH or NaOMe was added to PhH soln. of Pt complex;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824
反应条件
KOH or NaOMe in benzene alcoholic soln. of KOH or NaOMe was added to PhH soln. of Pt complex;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824
反应条件
KOH or NaOMe in benzene alcoholic soln. of KOH or NaOMe was added to PhH soln. of Pt complex;
参考文献
Goel, Ram G.; Ogiri, William O.; Srivastava, Ramesh C.
Organometallics, 1982 , vol. 1, p. 819 - 824