反应条件
K#Hg in tetrahydrofuran
stirring overnight under N2; the soln. siphoned off, the solvent removed in vac., the residue extd. with pentane, cooling to -80°C, the solvent siphoned off, the crystals washed with pentane, recrystn. from pentane and drying in vac.; elem. anal.;
参考文献
Mann, Brian E.; Musco, Alfredo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 776 - 785