反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 h 2: palladium hydroxide on carbon; hydrogen / ethyl acetate / 16 h / 20 °C 3: C50H73O4P / dichloromethane / 240 h / 5 °C / |Inert atmosphere 4: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C View Scheme
参考文献
Qabaja, Ghassan; Wilent, Jennifer E.; Benavides, Amanda R.; Bullard, George E.; Petersen, Kimberly S.
Organic Letters, 2013 , vol. 15, # 6 p. 1266 - 1269
