Gottumukkala, Aditya L.; Matcha, Kiran; Lutz, Martin; De Vries, Johannes G.; Minnaard, Adriaan J.
Chemistry - A European Journal, 2012 , vol. 18, # 22 p. 6907 - 6914
1: With 4 A molecular sieve; Rh2[N-benzene-fused phthaloyl-(S)-piperidinonate]4 in toluene T=-23°C; Mukaiyama aldol reaction; 12 h; 2: With hydrogenchloride in tetrahydrofuran T=23°C; 0.5 h; 3: With hydrogen; palladium on activated charcoal in methanol T=20°C; 2 h; Title compound not separated from byproducts;
1: With 4 A molecular sieve; Rh2[N-benzene-fused phthaloyl-(S)-piperidinonate]4 in toluene T=-23°C; Mukaiyama aldol reaction; 12 h; 2: With hydrogenchloride in tetrahydrofuran T=23°C; 0.5 h; 3: With hydrogen; palladium on activated charcoal in methanol T=20°C; 2 h; Title compound not separated from byproducts;