反应条件
1: pentanal tert-butylimine With lithium diethylamide in tetrahydrofuran; hexane
T=-10 - 0°C;
2: α-benzyloxyacetaldehyde in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane
T=-70 - 0°C;
3: With hydrogenchloride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane
T=20°C; 3.5 h;
参考文献
Grigorieva, N. Ya.; Tsiklauri, P. G.
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 665 - 670
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 3 p. 635 - 639
