Grigorieva, N. Ya.; Tsiklauri, P. G.
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 665 - 670
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 3 p. 635 - 639
1.1: lithium diethylamide / tetrahydrofuran; hexane / -10 - 0 °C
1.2: tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / -70 - 0 °C
1.3: 61 percent / hydrochloric acid / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 3.5 h / 20 °C
2.1: 94 percent / sodium borohydride
3.1: pyridine-sulfur trioxide / tetrahydrofuran / 3 h / 0 °C
3.2: 67 percent / LiAlH4 / tetrahydrofuran / 25 h
View Scheme
参考文献
Grigorieva, N. Ya.; Tsiklauri, P. G.
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 665 - 670
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 3 p. 635 - 639
1: diethyl (2-oxopropyl)phosphonate With potassium carbonate in ethanol
T=20°C; 2 h;
2: α-benzyloxyacetaldehyde in ethanol
T=20°C; 10 h;
参考文献
Munos, Jeffrey W.; Pu, Xiaotao; Mansoorabadi, Steven O.; Kim, Hak Joong; Liu, Hung-Wen
Journal of the American Chemical Society, 2009 , vol. 131, p. 2048 - 2049
Grubb's 2nd generation catalyst in dichloromethane
T=0 - 20°C;
参考文献
Lifchits, Olga; Mahlau, Manuel; Reisinger, Corinna M.; Lee, Anna; Fares, Christophe; Polyak, Iakov; Gopakumar, Gopinadhanpillai; Thiel, Walter; List, Benjamin
Journal of the American Chemical Society, 2013 , vol. 135, # 17 p. 6677 - 6693
