(Z)-2-乙酰氨基-3-苯基丙烯酸甲酯合成路线 (共 37 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tributyl-amine; lithium chloride; palladium diacetate in N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
Arcadi; Cacchi; Marinelli; Morera; Ortar
Tetrahedron, 1990 , vol. 46, # 20 p. 7151 - 7164
反应条件
hydrogenchloride in dichloromethane T=20°C; 20 h;
参考文献
Griesbeck, Axel G.; Bondock, Samir; Lex, Johann
Journal of Organic Chemistry, 2003 , vol. 68, # 26 p. 9899 - 9906
反应条件
potassium carbonate; C40H45O2N2P2PdCl2 in toluene T=140°C; Heck coupling reaction; 4 h;
参考文献
Krishna, Thatavarathy Rama; Jayaraman, Narayanaswamy
Tetrahedron, 2004 , vol. 60, # 45 p. 10325 - 10334
反应条件
sodium hydroxide in tetrahydrofuran 4 h;
参考文献
Barluenga, Jose; Ferrero, Miguel; Palacios, Francisco
Tetrahedron Letters, 1990 , vol. 31, # 24 p. 3497 - 3500
反应条件
sodium methylate T=20°C; 0.25 h;
参考文献
Jursic, Branko S.; Sagiraju, Sarada; Ancalade, Dustin K.; Clark, Traneil; Stevens, Edwin D.
Synthetic Communications, 2007 , vol. 37, # 10 p. 1709 - 1714
反应条件
triethylamine; triphenylphosphine in acetonitrile T=20°C; Wittig reaction; 24 h;
参考文献
Monatshefte fur Chemie, , vol. 135, # 7 p. 807 - 815
反应条件
potassium carbonate in acetone 1 h; Heating;
参考文献
Kitamura, Masato; Tsukamoto, Masaki; Bessho, Yuhki; Yoshimura, Masahiro; Kobs, Uwe; Widhalm, Michael; Noyori, Ryoji
Journal of the American Chemical Society, 2002 , vol. 124, # 23 p. 6649 - 6667
反应条件
potassium hydroxide in benzene T=40°C; ultrasound irradiation;
参考文献
Rajaram, S.; Lalitha, N.; Iyengar, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 9 p. 761 - 763
反应条件
potassium carbonate in acetone 6 h; Inert atmosphereSchlenk techniqueReflux;
参考文献
Frank, Dominik J.; Franzke, Axel; Pfaltz, Andreas
Chemistry - A European Journal, 2013 , vol. 19, # 7 p. 2405 - 2415
反应条件
potassium carbonate in acetone 1 h; Heating;
参考文献
Kitamura, Masato; Tsukamoto, Masaki; Bessho, Yuhki; Yoshimura, Masahiro; Kobs, Uwe; Widhalm, Michael; Noyori, Ryoji
Journal of the American Chemical Society, 2002 , vol. 124, # 23 p. 6649 - 6667