(Z)-2-乙酰氨基-3-苯基丙烯酸甲酯合成路线 （共 37 条）
反应条件
1: C17H18NO6P With sodium hydride; sodium iodide in tetrahydrofuran; mineral oil T=0°C; 0.166667 h; Inert atmosphere; 2: benzaldehyde in tetrahydrofuran; mineral oil T=-78 - 0°C; 3.08333 h; Inert atmosphere; Overall yield = 72 percent; stereoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 10 p. 1884 - 1888
反应条件
in methanol; diethyl ether; toluene T=20°C; 0.5 h; Inert atmosphere;
参考文献
Guisado-Barrios, Gregorio; Munoz, Bianca K.; Kamer, Paul C. J.; Lastdrager, Bas; Van Der Marel, Gijs; Overhand, Mark; Vega-Vazquez, Marino; Martin-Pastor, Manuel
Dalton Transactions, 2013 , vol. 42, # 6 p. 1973 - 1978
反应条件
1-methyl-pyrrolidin-2-one; phenylmethyltriethylammonium bromide; N-ethyl-N,N-diisopropylamine; [Pd02(E,E-dibenzylideneacetone-3,3',5,5'-OMe)3] T=125°C; Heck reaction; 3 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 34 p. 8750 - 8761
反应条件
1: 80 percent / phosphorus pentaoxide / CHCl3 / 24 h / Heating 2: benzene / 24 h / 10 °C / UV-irradiation 3: 70 percent / hydrochloric acid / CH2Cl2 / 3 h / 20 °C 4: 80 percent / hydrochloric acid / CH2Cl2 / 20 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 26 p. 9899 - 9906
反应条件
1: benzene / 24 h / 10 °C / UV-irradiation 2: 70 percent / hydrochloric acid / CH2Cl2 / 3 h / 20 °C 3: 80 percent / hydrochloric acid / CH2Cl2 / 20 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 26 p. 9899 - 9906
反应条件
1: 97 percent / benzene / 6 h / Ambient temperature 2: 88 percent / 2N NaOH / tetrahydrofuran / 4 h View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 24 p. 3497 - 3500
反应条件
in methanol; diethyl ether T=-0.15°C;
参考文献
Journal of Organometallic Chemistry, , vol. 689, # 4 p. 751 - 758
反应条件
3: 64 percent / K2CO3, 30percent H2O2 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Liebigs Annalen der Chemie, , # 8 p. 1469 - 1475
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 977 - 980
反应条件
1: SOCl2 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 83, # 1 p. 258 - 277
