(Z)-2-乙酰氨基-3-苯基丙烯酸甲酯合成路线 （共 37 条）
反应条件
hydrogen; tetrafluoroboric acid; Rh complex from Rh(COD)acac; (R,R)-4,5-bis(diphenylphosphinomethyl)-2-methyl-2-phenyl-1,3-dioxolane P=760 Torr; Title compound not separated from byproducts;
参考文献
Boerner, Armin; Holz, Jens; Kless, Achim; Heller, Detlef; Berens, Ulrich
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6071 - 6074
反应条件
hydrogen; norborna-2,5-diene(S,S-1,2-bis(2,5-diethylphospholanyl)benzene)rhodium(I) tetrafluoroborate in ethanol T=26°C; P=2250.18 Torr; Kinetics; Further Variations:Catalysts;
参考文献
Cobley, Christopher J; Lennon, Ian C; McCague, Raymond; Ramsden, James A; Zanotti-Gerosa, Antonio
Tetrahedron Letters, 2001 , vol. 42, # 42 p. 7481 - 7483
反应条件
hydrogen; tetrafluoroboric acid; Rh complex from Rh(COD)acac; (R,R)-4,5-bis(diphenylphosphinomethyl)-2-methyl-2-phenyl-1,3-dioxolane P=760 Torr; Title compound not separated from byproducts;
参考文献
Boerner, Armin; Holz, Jens; Kless, Achim; Heller, Detlef; Berens, Ulrich
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6071 - 6074
反应条件
in methanol; diethyl ether
96 h; Ambient temperature;
参考文献
Cativiela, Carlos; Villegas, Maria D. Diaz de; Mayoral, Jose A.; Melendez, Enrique
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3167 - 3169
反应条件
1: CHCl3 / 72 h / Ambient temperature
2: BF3*Et2O / 0.25 h / Heating
3: 10percent KOH / methanol / 0.5 h / 65 °C
View Scheme
参考文献
Catiela, Carlos; Villegas, M. Dolores Diaz de; Gainza, M. Pilar
Synthetic Communications, 1987 , vol. 17, # 2 p. 165 - 172
反应条件
1: 100 percent / diethyl ether; CHCl3 / 72 h / Ambient temperature
2: 80 percent / ethane-1,2-diol / 0.17 h / 200 °C
View Scheme
参考文献
Cativiela, C.; Diaz de Villegas, M. D.; Melendez, E.
Synthesis, 1986 , # 5 p. 418 - 419
反应条件
trichlorophosphate in dichloromethane
T=60°C; Bischler-Napieralski reaction; 2 h;
参考文献
Griesbeck, Axel G.; Bondock, Samir; Lex, Johann
Journal of Organic Chemistry, 2003 , vol. 68, # 26 p. 9899 - 9906
