1-甲基-1H-吲哚-2-甲腈合成路线 (共 17 条)
反应条件
in xylene
16 h; Heating;
参考文献
Fang, Jim-Min; Yang,Chau-Chen; Wang, Yu-Wen
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 477 - 481
反应条件
in methanol
10 h; electochemical reaction;
参考文献
Lin, Chih-Da; Fang, Jim-Min
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1993 , vol. 40, # 6 p. 571 - 580
反应条件
1: hydroxylamine hydrochloride; pyridine / ethanol / 2 h / 90 °C
2: triethylamine / 2 h / 90 °C
View Scheme
参考文献
MIIKANA THERAPEUTICS, INC.
Patent: WO2008/154026 A1, 2008 ;
WO 2008/154026 A1
反应条件
2: 28 percent / xylene / 16 h / Heating
View Scheme
参考文献
Fang, Jim-Min; Yang,Chau-Chen; Wang, Yu-Wen
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 477 - 481
反应条件
in methanol
12 h; electrochemical reaction; var. oxidative potentials, initial current and time; Product distribution;
参考文献
Lin, Chih-Da; Fang, Jim-Min
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1993 , vol. 40, # 6 p. 571 - 580
反应条件
benzenethiol sodium salt in tetrahydrofuran
T=68°C; 72 h;
参考文献
Lin, Chih-Da; Fang, Jim-Min
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1993 , vol. 40, # 6 p. 571 - 580
反应条件
in diethyl ether
T=-40 - 20°C; 16 h;
参考文献
Lin, Chih-Da; Fang, Jim-Min
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1993 , vol. 40, # 6 p. 571 - 580