1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h; regioselective reaction;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
(η5-C5H5)Fe(CO)2Me in N,N-dimethyl-formamide Bu2GeH2 was treated with Et3SiH (2 equiv.) in DMF in presence of Fe catalyst at 100°C for 24 h in sealed tube;
1: With trichlorophosphate in anhydrous dichloroethane Vilsmeier-Haack reaction; 1 h; Reflux; 2: With potassium hydroxide in anhydrous dichloroethane; water 0.0166667 h; regioselective reaction;
参考文献
Ilyin, Petrv.; Pankova, Alenas.; Kuznetsov, Mikhail A.
Synthesis, 2012 , vol. 44, # 9 p. 1353 - 1358
