α,β-二邻苯二甲酰亚胺基乙烷合成路线 (共 24 条)
反应条件
sodium carbonate
T=25°C; 170 h;
参考文献
Kadam, A. N.; Ghatge, B. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 460 - 461
参考文献
Teramura et al.
Kogyo Kagaku Zasshi, 1954 , vol. 57, p. 405
Chem.Abstr., 1955 , p. 15734
反应条件
in acetone
T=10 - 20°C; 0.833333 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al.
Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118
反应条件
1: 92 percent / acetonitrile / 0.08 h / Ambient temperature
2: 96 percent / Heating
View Scheme
参考文献
Guirado, Antonio; Zapata, Andres; Ramirez De Arellano, M. Carmen
Tetrahedron, 1997 , vol. 53, # 14 p. 5305 - 5324
参考文献
Sakellarios
Helvetica Chimica Acta, 1946 , vol. 29, p. 1675,1677, 1681
反应条件
8.5 h; Ambient temperatureIrradiation;
参考文献
Takechi, Haruko; Machida, Minoru; Kanaoka,Yuichi
Liebigs Annalen der Chemie, 1986 , # 5 p. 859 - 868
参考文献
Balaban
Journal of the Chemical Society, 1926 , p. 572
反应条件
1: dimethylformamide / 6 h / 180 °C
2: 8 percent / acetone / 16 h / 10 - 20 °C / Irradiation
View Scheme
参考文献
Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al.
Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118
反应条件
xylene
unter Abdestillieren des Loesungsmittels und weiteren Erhitzen bis auf 200grad;
参考文献
Sakellarios
Helvetica Chimica Acta, 1946 , vol. 29, p. 1675,1677, 1681
参考文献
Jocelyn
Journal of the Chemical Society, 1957 , p. 3305