1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 0 °C / |Inert atmosphere
1.2: 2 h / 0 - 20 °C / |Inert atmosphere
2.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / N,N-dimethyl acetamide / 7 h / 140 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
De, Subhadip; Chaudhuri, Saikat; Mishra, Sourabh; Mamtani, Himanshu; Bisai, Alakesh
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1871 - 1884
1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 0 °C / |Inert atmosphere
1.2: 2 h / 0 - 20 °C / |Inert atmosphere
2.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / N,N-dimethyl acetamide / 7 h / 140 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
De, Subhadip; Chaudhuri, Saikat; Mishra, Sourabh; Mamtani, Himanshu; Bisai, Alakesh
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1871 - 1884