4-[1-(苯基硫代)乙基]苯甲醚合成路线 (共 5 条)
反应条件
potassium carbonate in 1,4-dioxane
T=110°C; 24 h; Inert atmosphere;
参考文献
Ding, Qiuping; Cao, Banpeng; Yuan, Jianjun; Liu, Xianjin; Peng, Yiyuan
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 3 p. 748 - 751
反应条件
triethylsilane; indium tribromide in toluene
T=100°C; 1 h; Inert atmosphere;
参考文献
Sakai, Norio; Moritaka, Kohei; Konakahara, Takeo
European Journal of Organic Chemistry, 2009 , # 24 p. 4123 - 4127
反应条件
anhydrous iron chloride; AgNTf2 in 1,4-dioxane
T=80°C; 24 h; regioselective reaction;
参考文献
Cabrero-Antonino, Jose R.; Leyva-Perez, Antonio; Corma, Avelino
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 678 - 687
反应条件
1: 1,4-dioxane / 24 h / 80 °C
2: anhydrous iron chloride; AgNTf2 / 1,4-dioxane / 24 h / 80 °C
View Scheme
参考文献
Cabrero-Antonino, Jose R.; Leyva-Perez, Antonio; Corma, Avelino
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 678 - 687
反应条件
1: 4-methoxy-α-methylbenzyl alcohol With iodine; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=20°C; 0.5 h;
2: thiophenol T=20°C;
参考文献
Yadav, Lal Dhar S.; Garima; Kapoor, Ritu
Synthetic Communications, 2011 , vol. 41, # 1 p. 100 - 112